Laboratory Solutions for Material Science
 
  
 
 

OCA 30 / OCAH 230 Video-Based Semi-Automatic Contact Angle 

Description:
Contact angle measuring device for the semi-automatic measurement of the wetting behavior of solids, as well as for series tests and systematic analysis. The OCA 30 enables the reduction of subjective factors and time involved for contact angle measurements in research, quality- and production inspection.

Typical fields of application: 

For the software-controlled measurement and analysis of

  • the static and dynamic contact angle according to the Sessile and Captive Drop method 
  • the drop shape according to the Pendant Drop method 
  • the wetting behavior on solid surfaces 
  • the surface free energy of solids and their components 
  • the surface and interfacial tension out of the analysis of the drop shape

Equipment:

The OCA 30 consists of the basic instrument with the following technical equipment:

  • Dosing bay for installation of the optional manual syringe units and single or multiple (max. 4, optional 6) needle support with a vertical and horizontal fine adjustment 
  • Measuring stage software controlled motorized adjustable in Y- and Z- axis adjustable for accurate sample positioning and drop pick up from the dosing needle, in X-axis manual adjustable 
  • Lens mount with adjustable tilt 
  • High-performance six-fold power zoom lens with an integrated continuous fine focus 
  • High-speed video system with adapter and CCD-camera 
  • High-performance video digitizing board (frame grabber) for the PC 
  • Halogen lighting with continuously adjustable intensity without hysteresis for a homogeneous back lighting 
  • Control and measuring electronics with built-in digital temperature display and serial RS 232C interface 
  • Power supply with automatic voltage adjustment 

Features of performance:

The 32-bit software SCA 20 developed for Windows XP/2000/NT offers by various expansion steps:
  • Control of the sample position in Y- and Z-direction, the electronic syringe modules, the tilting base assemblies, wafer stages and temperature control units 
  • Static and dynamic contact angle measurement according to the Sessile and Captive Drop method 
  • Calculation of the surface and interfacial tension from the contours of pendant and sessile drops as well as of liquid lamellas on plates, rods and threads 
  • Calculation of the surface free energy of solids and their components (e.g. dispersion, polar and hydrogen bond force contribution, acid and base portions respectively) according to the theories of Wu, Zisman, Owens-Wendt, Extended Fowkes, Schultz 1 + 2, Fowkes, van Oss & Good (Acid-Base), Equation of States (EOS) 
  • Calculation of wetting envelopes from the surface free energy
  • Statistics and measurement error analysis

Technical Data:
 
Maximum sample size (L x W x H) : 220 x x 70 mm, 8"-Wafer on WT 200 M/E
Size of sample stage : 100 x 100 mm
Position accuracy  : ± 0.1 mm
Range of contact angle measurement : 0 … 180° ; ± 0.1° measuring accuracy of the video system
Range of surface and interfacial tension : 1·10-² … 2·10³ mN/m; resolution: min. ± 0.05 mN/m
Optics : Six-fold zoom lens (0.7 … 4.5-fold magnification) with integrated fine focus (±6 mm) and high light transmitting capacity.
CCD-camera with a resolution up to 1600 x 1240 pixels (768 x 576 pixels standard)
Field of view (FOV): 1.75 x 1.4 … 11.7 x 9 mm
Optical distortion: < 0.05 % 
Video system : High-performance image processing system with 132 MBytes/s data transfer rate (compatible to European standard CCIR and US standard RS-170) 
Up to 50 images/s digitizing speed (60 images/s with RS-170)
Measuring methods : Sessile and Captive Drop method
Tilting Plate/Base method
Pendant & Oscillating Drop method
Lamella method
Temperature measurement and range : 2x Pt100 input for -60 … 450 °C (Pt100 optional), 0.1 K resolution; 1/3 DIN IEC 751 (± 0.03 %), class B
Size of device (L x W x H) : 590 x 220 x 550 mm
Weight : 20 kg
Power supply : 100 … 240 VAC; 50 … 60 Hz; 80 VA
Alternative/Supplementary units and accessories : Manual and electrical single dosing units; manual and electrical multiple dosing units; manual and electrical wafer stages and tilting base assemblies; electrical tilting base unit; liquid, peltier and electrical temperature control units (-10 … 400 °C); suction plate; film sample holder; optical contact angle and surface tension standards; dosing needles; syringes; PTFE-tubes; temperature inert glass cells; complete PC systems


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